Synthesis and structure of K_2[HMo_6^V^IV^VO_2_2(NH_3CH_2COO)_3]ˇ8 H_2O: a new example of a polyoxomolybdovanadate coordinated by a glycinato ligand (CROSBI ID 89617)
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Podaci o odgovornosti
Cindrić, Marina ; Strukan, Neven ; Devčić, Maja ; Kamenar, Boris
engleski
Synthesis and structure of K_2[HMo_6^V^IV^VO_2_2(NH_3CH_2COO)_3]ˇ8 H_2O: a new example of a polyoxomolybdovanadate coordinated by a glycinato ligand
The K_2[HMo_6VO_2_2(NH_3CH_2COO)_3]8H_2O has been prepared from molybdenum(VI)-oxide and vanadium(V)-oxide in aqueous solution by adding glycine and potasium chloride, and its structure determined by X-ray structure analysis. The molybdovanadate anion is built up of six MoO_6 edge-sharing octahedra connected into a ring centred by VO_4 tetrahedron. The MoO_6 octahedra are in pairs linked by the bridging glycine-carboxylato ligands.
crystal structure; molybdovanadates; glycine; carboxylato ligand.
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