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Synthesis and structural character-ization of metallated bioconjugates: C-terminal labeling of amino acids with ferroceneamine (CROSBI ID 540541)

Prilog sa skupa u zborniku | izvorni znanstveni rad | međunarodna recenzija

Jios, Jorge L. ; Buceta, Norma N. ; Kirin, Srećko I. ; Metzler-Nolte, Nils ; Della Vedova, Carlos O. ; Weyhermüller, Thomas Synthesis and structural character-ization of metallated bioconjugates: C-terminal labeling of amino acids with ferroceneamine // Proceedings of ECSOC-10, The Tenth International Electronic Conference on Synthetic Organic Chemistry / Seijas, Julio A. ; Vazquez-Tato, M. Pilar (ur.). Basel: MDP International, 2006. str. c013/1-c013/10

Podaci o odgovornosti

Jios, Jorge L. ; Buceta, Norma N. ; Kirin, Srećko I. ; Metzler-Nolte, Nils ; Della Vedova, Carlos O. ; Weyhermüller, Thomas

engleski

Synthesis and structural character-ization of metallated bioconjugates: C-terminal labeling of amino acids with ferroceneamine

Ferroceneamine, H2N-Fc, has been substituted to the C-terminus of 6 amino acids using the HBTU / HOBt coupling protocol. The synthesized bioconjugates Boc-Aaa-Fc, Aaa = Gly (1), Leu (2), Phe (3), Val (4), Cys(Acm) (5), Tyr(tBu) (6) (Acm = acetamidomethyl, tBu = t-buthyl), have been characterized by 1H NMR, 13C NMR EI-MS, EI-HRMS, UV and CD spectroscopies. In addition, a VT NMR study on 4 and the X-ray structure of 1 are presented.

Amino acids; bioorganometallic chemistry; ferrocene; peptides; X-ray

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Podaci o prilogu

c013/1-c013/10.

2006.

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objavljeno

3-906980-18-9

Podaci o matičnoj publikaciji

Proceedings of ECSOC-10, The Tenth International Electronic Conference on Synthetic Organic Chemistry

Seijas, Julio A. ; Vazquez-Tato, M. Pilar

Basel: MDP International

Podaci o skupu

The Tenth International Electronic Conference on Synthetic Organic Chemistry

poster

01.11.2006-30.11.2006

internet

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