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Pentaerythritol crystallization - Influence of the process conditions on the granulometric properties of crystals (CROSBI ID 169210)

Prilog u časopisu | izvorni znanstveni rad | međunarodna recenzija

Sander, Aleksandra ; Prlić Kardum, Jasna Pentaerythritol crystallization - Influence of the process conditions on the granulometric properties of crystals // Advanced powder technology, 23 (2012), 2; 191-198. doi: 10.1016/j.apt.2011.02.001

Podaci o odgovornosti

Sander, Aleksandra ; Prlić Kardum, Jasna

engleski

Pentaerythritol crystallization - Influence of the process conditions on the granulometric properties of crystals

The quality of crystals depends on many factors that determine their granulometric properties. In order to obtain crystals of desired size distribution, proper selection of the operating conditions is of a great importance. Commonly, the unseeded cooling crystallization is controlled by selecting the appropriate cooling profile. The crystallization process can also be controlled by adding a certain number of seed crystals of a uniform size in the crystallizer at the saturation temperature. This paper investigates the influence of the process conditions (mixing intensity, cooling profile, batch time, saturation temperature and seeding) on the granulometric properties of pentaerythritol obtained by batch cooling crystallization. All investigated process conditions influences the crystal size distribution (seeded and unseeded experiments). On the other hand, the shape of crystals was the same for all experimental conditions. Optimal cooling profile, lower retention time, higher mixing rate and smaller initial seed surface area improves the final crystal size distribution.

crystallization ; granulometric properties ; pentaerythritol ; seeding

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Podaci o izdanju

23 (2)

2012.

191-198

objavljeno

0921-8831

1568-5527

10.1016/j.apt.2011.02.001

Povezanost rada

Kemijsko inženjerstvo

Poveznice
Indeksiranost