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3(S)-Acetoxymethyl-7-chloro-1, 3-dihydro-1-methyl-5-phenyl-2H-1, 4-benzodiazepin-2-one (CROSBI ID 93551)

Prilog u časopisu | izvorni znanstveni rad | međunarodna recenzija

Višnjevac, Aleksandar ; Avdagić, Amir ; Kojić-Prodić, Biserka 3(S)-Acetoxymethyl-7-chloro-1, 3-dihydro-1-methyl-5-phenyl-2H-1, 4-benzodiazepin-2-one // Acta crystallographica. Section E, Structure reports online, 58 (2002), 2; 148-150

Podaci o odgovornosti

Višnjevac, Aleksandar ; Avdagić, Amir ; Kojić-Prodić, Biserka

engleski

3(S)-Acetoxymethyl-7-chloro-1, 3-dihydro-1-methyl-5-phenyl-2H-1, 4-benzodiazepin-2-one

The enantiomerically pure (S) title compound, C19H17ClN2O3, was crystallized from a 1:1 mixture of ethanol and dichloromethane. The 1, 4-diazepine ring has a boat conformation with the C atom in position 3 displaced by 0.729 (4) Ĺ from the plane defined by the atoms in positions 1, 2, 4 and 5. A weak C-HO interaction, the most prominent feature of the crystal packing, links the molecules into infinite chains stretched along the c axis. The title compound, as well as other 1, 4-benzodiazepin-2-one derivatives, are suitable precursors for the synthesis of enantiomerically pure -amino acids and their congeners

1 ; 4-benzodiazepin-2-one

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Podaci o izdanju

58 (2)

2002.

148-150

objavljeno

1600-5368

Povezanost rada

Kemija