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Green and rapid mechanosynthesis of high-porosity NU- and UiO-type metal–organic frameworks (CROSBI ID 251655)

Prilog u časopisu | izvorni znanstveni rad | međunarodna recenzija

Fidelli, Athena M. ; Karadeniz, Bahar ; Howarth, Ashlee J. ; Huskić, Igor ; Germann, Luzia S. ; Halasz, Ivan ; Etter, Martin ; Moon, Su-Young ; Dinnebier, Robert E. ; Stilinović, Vladimir et al. Green and rapid mechanosynthesis of high-porosity NU- and UiO-type metal–organic frameworks // Chemical communications, 54 (2018), 51; 6999-7002. doi: 10.1039/c8cc03189d

Podaci o odgovornosti

Fidelli, Athena M. ; Karadeniz, Bahar ; Howarth, Ashlee J. ; Huskić, Igor ; Germann, Luzia S. ; Halasz, Ivan ; Etter, Martin ; Moon, Su-Young ; Dinnebier, Robert E. ; Stilinović, Vladimir ; Farha, Omar K. ; Friščić, Tomislav ; Užarević, Krunoslav

engleski

Green and rapid mechanosynthesis of high-porosity NU- and UiO-type metal–organic frameworks

The use of a dodecanuclear zirconium acetate cluster as a precursor enables the rapid, clean mechanochemical synthesis of high-microporosity metal–organic frameworks NU-901 and UiO-67, with surface areas up to 2250 m2 g−1. Real-time X-ray diffraction monitoring reveals that mechanochemical reactions involving the conventional hexanuclear zirconium methacrylate precursor are hindered by the formation of an inert intermediate, which does not appear when using the dodecanuclear acetate cluster as a reactant.

mechanochemical synthesis ; MOF materials ; NU-901 ; UiO-67

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Podaci o izdanju

54 (51)

2018.

6999-7002

objavljeno

1359-7345

1364-548X

10.1039/c8cc03189d

Povezanost rada

Kemija

Poveznice
Indeksiranost