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Synthesis, structural characterization and anion binding ability of sterically congested adamantane-calix[4]pyrroles and adamantane-calixphyrins (CROSBI ID 146200)

Prilog u časopisu | izvorni znanstveni rad | međunarodna recenzija

Alešković, Marija ; Halasz, Ivan ; Basarić, Nikola ; Mlinarić-Majerski, Kata Synthesis, structural characterization and anion binding ability of sterically congested adamantane-calix[4]pyrroles and adamantane-calixphyrins // Tetrahedron, 65 (2009), 10; 2051-2058. doi: 10.1016/j.tet.2009.01.007

Podaci o odgovornosti

Alešković, Marija ; Halasz, Ivan ; Basarić, Nikola ; Mlinarić-Majerski, Kata

engleski

Synthesis, structural characterization and anion binding ability of sterically congested adamantane-calix[4]pyrroles and adamantane-calixphyrins

Novel adamantane derivatives of calix[4]pyrrole 4-8 and calixphyrin 9 have been synthesized. The structure of 8 has been characterized by X-ray powder diffraction and the structure of 9 by single crystal X-ray analysis. Whereas calixphyrin 9 does not bind anions, analogous calyx[4]pyrrole 8 forms a complex with Cl- in the DMSO solution and in the solid state. The solid state complexation has been accomplished on grinding in a mill, which is the first example of complex formation with an anion in the solid state

adamantane-calix[4]pyrroles ; synthesis ; X-ray powder diffraction analysis ; anion binding

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Podaci o izdanju

65 (10)

2009.

2051-2058

objavljeno

0040-4020

1464-5416

10.1016/j.tet.2009.01.007

Povezanost rada

Kemija

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