Synthesis, structural characterization and anion binding ability of sterically congested adamantane-calix[4]pyrroles and adamantane-calixphyrins (CROSBI ID 146200)
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Alešković, Marija ; Halasz, Ivan ; Basarić, Nikola ; Mlinarić-Majerski, Kata
engleski
Synthesis, structural characterization and anion binding ability of sterically congested adamantane-calix[4]pyrroles and adamantane-calixphyrins
Novel adamantane derivatives of calix[4]pyrrole 4-8 and calixphyrin 9 have been synthesized. The structure of 8 has been characterized by X-ray powder diffraction and the structure of 9 by single crystal X-ray analysis. Whereas calixphyrin 9 does not bind anions, analogous calyx[4]pyrrole 8 forms a complex with Cl- in the DMSO solution and in the solid state. The solid state complexation has been accomplished on grinding in a mill, which is the first example of complex formation with an anion in the solid state
adamantane-calix[4]pyrroles ; synthesis ; X-ray powder diffraction analysis ; anion binding
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