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Pregled bibliografske jedinice broj: 636141

Časopis

Autori: Gembarovski, Dubravka; Gabelica Marković, Vesna; Galić, Nives
Naslov: Structural Elucidation Studies of 15-Membered Azalide Macrocycles using H/D Exchange and ESI-MSn
( Structural Elucidation Studies of 15-Membered Azalide Macrocycles using H/D Exchange and ESI-MSn )
Izvornik: Journal of pharmaceutical and biomedical analysis (0731-7085) 86 (2013); 1-10
Vrsta rada: članak
Ključne riječi: 15-Membered Azalide Aglycone; macrolides; ESI-MSn; H/D exchange; fragmentation; sodium adducts
( 15-Membered Azalide Aglycone; macrolides; ESI-MSn; H/D exchange; fragmentation; sodium adducts )
Sažetak:
A comprehensive study of fragmentation pathways of 15-membered azalide macrocycles using electrospray ionisation with multistage mass spectrometry (ESI-MSn) is presented in this work. Hydrogen/deuterium (H/D) exchange experiments and high-resolution mass spectrometry were used to investigate the proposed fragmentation pathways. In addition, the fragmentation patterns of sodium adduct ions [M+Na]+ of the macrocycles were also investigated as the presence of an alkali metal interacting with the aglycone ring influences the product-ion spectra.
Projekt / tema: 119-1191342-1083, 119-1191342-2960
Izvorni jezik: eng
Rad je indeksiran u
bazama podataka:
Current Contents Connect (CCC)
MEDLINE
Scopus
SCI-EXP, SSCI i/ili A&HCI
Science Citation Index Expanded (SCI-EXP) (sastavni dio Web of Science Core Collectiona)
Kategorija: Znanstveni
Znanstvena područja:
Kemija
URL Internet adrese: http://dx.doi.org/10.1016/j.jpba.2013.07.011
http://ac.els-cdn.com/S0731708513003075/1-s2.0-S0731708513003075-main.pdf?_tid=c469c926-f16f-11e3-9d4e-00000aacb360&acdnat=1402494989_7fb33e60ce405bcfaebdd1566d2151df
http://www.sciencedirect.com/science/article/pii/S0731708513003075
Broj citata:
Altmetric:
DOI: 10.1016/j.jpba.2013.07.011
URL cjelovitog teksta: http://dx.doi.org/10.1016/j.jpba.2013.07.011
Google Scholar: Structural Elucidation Studies of 15-Membered Azalide Macrocycles using H/D Exchange and ESI-MSn
Upisao u CROSBI: Nives Galić (ngalic@chem.pmf.hr:Nives.Galic@chem.pmf.hr), 8. Srp. 2013. u 12:02 sati



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